Synthesis and Diels−Alder Reactions of 1,2-Dimethylene[2.<i>n</i>]metacyclophanes

The Diels−Alder reaction of 1,2-dimethylene[2.n]MCPs (MCP = metacyclophane) with suitable dienophiles followed by aromatization and photoinduced or FeCl3-induced transannular cyclization afforded phenanthrene-anellated polycyclic aromatic hydrocarbons, which were found to adopt helical chirality in the solid state.

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PID https://www.doi.org/10.1021/ol0483403.s002
URL http://dx.doi.org/10.1021/ol0483403.s002
URL https://figshare.com/articles/Synthesis_and_Diels_Alder_Reactions_of_1_2_Dimethylene_2_i_n_i_metacyclophanes/3305872
URL https://figshare.com/articles/dataset/Synthesis_and_Diels_Alder_Reactions_of_1_2_Dimethylene_2_i_n_i_metacyclophanes/3305872
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Author Yamato, Takehiko
Author Miyamoto, Shinpei
Author Hironaka, Tohru
Author Miura, Yoshinori
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Collected From figshare
Hosted By figshare
Publication Date 2016-01-01
Publisher Figshare
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Language UNKNOWN
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Source https://science-innovation-policy.openaire.eu/search/dataset?datasetId=r37980778c78::283e94b4a401c7a6d6c83c593c4dd9d9
Author jsonws_user
Last Updated 16 December 2020, 06:20 (CET)
Created 16 December 2020, 06:20 (CET)