Asymmetric Crystallization of an Achiral Lariat-type Macrocyclic Compound

The first example of a macrocyclic lariat-type compound 3, which, despite being achiral in solution, undergoes asymmetric crystallization and enantiomeric excess, was observed for a sample of ground crystals. Among 32 independent crystallizations, in 23 cases of samples an enantiomeric excess was observed; furthermore six of these included a vast majority of one enantiomer.

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PID https://www.doi.org/10.1021/cg050325x.s004
PID https://www.doi.org/10.1021/cg050325x.s003
URL https://figshare.com/articles/dataset/Asymmetric_Crystallization_of_an_Achiral_Lariat_type_Macrocyclic_Compound/3245908
URL https://figshare.com/articles/Asymmetric_Crystallization_of_an_Achiral_Lariat_type_Macrocyclic_Compound/3245899
URL https://figshare.com/articles/Asymmetric_Crystallization_of_an_Achiral_Lariat_type_Macrocyclic_Compound/3245908
URL https://figshare.com/articles/dataset/Asymmetric_Crystallization_of_an_Achiral_Lariat_type_Macrocyclic_Compound/3245899
URL http://dx.doi.org/10.1021/cg050325x.s003
URL http://dx.doi.org/10.1021/cg050325x.s004
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Access Right Open Access
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Author Kalisiak, Jarosław
Author Jurczak, Janusz
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Collected From figshare
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Publication Date 2016-01-01
Publisher Figshare
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Language UNKNOWN
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Source https://science-innovation-policy.openaire.eu/search/dataset?datasetId=dedup_wf_001::b8ac8a15efbfa58a749abc5f8fa095a8
Author jsonws_user
Last Updated 16 December 2020, 09:36 (CET)
Created 16 December 2020, 09:36 (CET)